Principles of Instrumental Analysis

Höfundar: Douglas A. Skoog, F. James Holler, Stanley R. Crouch

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PRINCIPLES OF INSTRUMENTAL ANALYSIS is the standard for courses on the principles and applications of modern analytical instruments. In the 7th edition, authors Skoog, Holler, and Crouch infuse their popular text with updated techniques and several new Instrumental Analysis in Action case studies. Updated material enhances the book's proven approach, which places an emphasis on the fundamental principles of operation for each type of instrument, its optimal area of application, its sensitivity, its precision, and its limitations.

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Höfundar: Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Útgáfa:7
Útgáfudagur: 2017-01-01
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Format:Page Fidelity
ISBN 13: 9781337468039
Print ISBN: 9781305577213
ISBN 10: 1337468037

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Contents Overview
Contents
Preface
Chapter 1: Introduction
- 1A Classification of Analytical Methods
- 1B Types of Instrumental Methods
- 1C Instruments for Analysis
- 1D Calibration of Instrumental Methods
- 1E Selecting an Analytical Method
- Questions and Problems
Section 1: Measurement Basics
- Chapter 2: Electrical Components and Circuits
  - 2A Direct-Current Circuits and Measurements
  - 2B Alternating Current Circuits
  - 2C Semiconductors and Semiconductor Devices
  - 2D Power Supplies and Regulators
  - 2E Readout Devices
  - Questions and Problems
- Chapter 3: Operational Amplifiers in Chemical Instrumentation
  - 3A Properties of Operational Amplifiers
  - 3B Operational Amplifier Circuits
  - 3C Amplification and Measurement of Transducer Signals
  - 3D Application of Operational Amplifiers to Voltage and Current Control
  - 3E Application of Operational Amplifiers to Mathematical Operations
  - 3F Applications of Operational Amplifiers to Comparison
  - Questions and Problems
- Chapter 4: Digital Electronics and Computers
  - 4A Analog and Digital Signals
  - 4B Counting and Arithmetic with Binary Numbers
  - 4C Basic Digital Circuits
  - 4D Computers and Computerized Instruments
  - 4E Components of a Computer
  - 4F Computer Software
  - 4G Applications of Computers
  - 4H Computer Networks
  - Questions and Problems
- Chapter 5: Signals and Noise
  - 5A The Signal-to-Noise Ratio
  - 5B Sources of Noise in Instrumental Analyses
  - 5C Signal-to-Noise Enhancement
  - Questions and Problems
  - Instrumental Analysis in Action - The Electronic Analytical Laboratory
Section 2: Atomic Spectroscopy
- Chapter 6: An Introduction to Spectrometric Methods
  - 6A General Properties of Electromagnetic Radiation
  - 6B Wave Properties of Electromagnetic Radiation
  - 6C Quantum-Mechanical Properties of Radiation
  - 6D Quantitative Aspects of Spectrochemical Measurements
  - Questions and Problems
- Chapter 7: Components of Optical Instruments
  - 7A General Designs of Optical Instruments
  - 7B Sources of Radiation
  - 7C Wavelength Selectors
  - 7D Sample Containers
  - 7E Radiation Transducers
  - 7F Signal Processors and Readouts
  - 7G Fiber Optics
  - 7H Types of Optical Instruments
  - 7I Principles of Fourier Transform Optical Measurements
  - Questions and Problems
- Chapter 8: An Introduction to Optical Atomic Spectrometry
  - 8A Optical Atomic Spectra
  - 8B Atomization Methods
  - 8C Sample-Introduction Methods
  - Questions and Problems
- Chapter 9: Atomic Absorption and Atomic Fluorescence Spectrometry
  - 9A Sample Atomization Techniques
  - 9B Atomic Absorption Instrumentation
  - 9C Interferences in Atomic Absorption Spectroscopy
  - 9D Atomic Absorption Analytical Techniques
  - 9E Atomic Fluorescence Spectroscopy
  - Questions and Problems
- Chapter 10: Atomic Emission Spectrometry
  - 10A Emission Spectroscopy Based on Plasma Sources
  - 10B Emission Spectroscopy Based on Arc and Spark Sources
  - 10C Other Sources for Optical Emission Spectroscopy
  - Questions and Problems
- Chapter 11: Atomic Mass Spectrometry
  - 11A Some General Features of Atomic Mass Spectrometry
  - 11B Mass Spectrometers
  - 11C Inductively Coupled Plasma Mass Spectrometry
  - 11D Spark Source Mass Spectrometry
  - 11E Glow-Discharge Mass Spectrometry
  - 11F Other Mass Spectrometric Methods
  - Questions and Problems
- Chapter 12: Atomic X-ray Spectrometry
  - 12A Fundamental Principles
  - 12B Instrument Components
  - 12C X-ray Fluorescence Methods
  - 12D X-ray Absorption Methods
  - 12E The Electron Microprobe
  - Questions and Problems
  - Instrumental Analysis in Action - Monitoring Mercury
Section 3: Molecular Spectroscopy
- Chapter 13: An Introduction to Ultraviolet-Visible Molecular Absorption Spectrometry
  - 13A Measurement of Transmittance and Absorbance
  - 13B Beer's Law
  - 13C The Effects of Instrumental Noise on Spectrophotometric Analyses
  - 13D Instrumentation
  - Questions and Problems
- Chapter 14: Applications of Ultraviolet-Visible Molecular Absorption Spectrometry
  - 14A The Magnitude of Molar Absorptivities
  - 14B Absorbing Species
  - 14C Qualitative Applications of Ultraviolet Visible Absorption Spectroscopy
  - 14D Quantitative Analysis by Absorption Measurements
  - 14E Photometric and Spectrophotometric Titrations
  - 14F Spectrophotometric Kinetic Methods
  - 14G Spectrophotometric Studies of Complex Ions
  - Questions and Problems
- Chapter 15: Molecular Luminescence Spectrometry
  - 15A Theory of Fluorescence and Phosphorescence
  - 15B Fluorescence and Phosphorescene Instrumentation
  - 15C Applications of Photoluminescence Methods
  - 15D Chemiluminescence
  - Questions and Problems
- Chapter 16: An Introduction to Infrared Spectrometry
  - 16A Theory of IR Absorption Spectrometry
  - 16B IR Instrumentation
  - 16C IR Sources and Transducers
  - Questions and Problems
- Chapter 17: Applications of Infrared Spectrometry
  - 17A Mid-IR Absorption Spectrometry
  - 17B Mid-IR Reflection Spectrometry
  - 17C Photoacoustic IR Spectroscopy
  - 17D Near-IR Spectroscopy
  - 17E Far-IR Spectroscopy
  - 17F IR Emission Spectroscopy
  - 17G IR Microscopy and Imaging
  - Questions and Problems
- Chapter 18: Raman Spectroscopy
  - 18A Theory of Raman Spectroscopy
  - 18B Instrumentation
  - 18C Applications of Raman Spectroscopy
  - 18D Other Types of Raman Spectroscopy
  - Questions and Problems
- Chapter 19: Nuclear Magnetic Resonance Spectroscopy
  - 19A Theory of NMR
  - 19B Environmental Effects on NMR Spectra
  - 19C NMR Spectrometers
  - 19D Applications of Proton NMR
  - 19E Carbon-13 NMR
  - 19F Application of NMR to Other Nuclei
  - 19G Multiple Pulse and Multidimensional NMR
  - 19H Magnetic Resonance Imaging
  - Questions and Problems
- Chapter 20: Molecular Mass Spectrometry
  - 20A Molecular Mass Spectra
  - 20B Ion Sources
  - 20C Mass Spectrometers
  - 20D Applications of Molecular Mass Spectrometry
  - 20E Quantitative Applications of Mass Spectrometry
  - Questions and Problems
- Chapter 21: Surface Characterization by Spectroscopy and Microscopy
  - 21A Introduction to the Study of Surfaces
  - 21B Spectroscopic Surface Methods
  - 21C Electron Spectroscopy
  - 21D Ion Spectroscopic Techniques
  - 21E Surface Photon Spectroscopic Methods
  - 21F Electron-Stimulated Microanalysis Methods
  - 21G Scanning Probe Microscopes
  - Questions and Problems
  - Instrumental Analysis in Action - Assessing the Authenticity of the Vinland Map: Surface Analysis in
Section 4: Electroanalytical Chemistry
- Chapter 22: An Introduction to Electroanalytical Chemistry
  - 22A Electrochemical Cells
  - 22B Potentials in Electroanalytical Cells
  - 22C Electrode Potentials
  - 22D Calculation of Cell Potentials from Electrode Potentials
  - 22E Currents in Electrochemical Cells
  - 22F Types of Electroanalytical Methods
  - Questions and Problems
- Chapter 23: Potentiometry
  - 23A General Principles
  - 23B Reference Electrodes
  - 23C Metallic Indicator Electrodes
  - 23D Membrane Indicator Electrodes
  - 23E Ion-Selective Field-Effect Transistors
  - 23F Molecular-Selective Electrode Systems
  - 23G Instruments for Measuring Cell Potentials
  - 23H Direct Potentiometric Measurements
  - 23I Potentiometric Titrations
  - Questions and Problems
- Chapter 24: Coulometry
  - 24A Current-Voltage Relationships during an Electrolysis
  - 24B An Introduction to Coulometric Methods of Analysis
  - 24C Controlled-Potential Coulometry
  - 24D Coulometric Titrations
  - Questions and Problems
- Chapter 25: Voltammetry
  - 25A Excitation Signals in Voltammetry
  - 25B Voltammetric Instrumentation
  - 25C Hydrodynamic Voltammetry
  - 25D Cyclic Voltammetry
  - 25E Pulse Voltammetry
  - 25F High-Frequency and High-Speed Voltammetry
  - 25G Applications of Voltammetry
  - 25H Stripping Methods
  - 25I Voltammetry with Microelectrodes
  - Questions and Problems
  - Instrumental Analysis in Action - Measuring the Parts to Understand the Whole: The Microphysiometer
Section 5: Separation Methods
- Chapter 26: An Introduction to Chromatographic Separations
  - 26A General Description of Chromatography
  - 26B Migration Rates of Solutes
  - 26C Band Broadening and Column Efficiency
  - 26D Optimization of Column Performance
  - 26E Summary of Chromatographic Relationships
  - 26F Applications of Chromatography
  - Questions and Problems
- Chapter 27: Gas Chromatography
  - 27A Principles of GLC
  - 27B Instruments for GLC
  - 27C Gas Chromatographic Columns and Stationary Phases
  - 27D Applications of GC
  - 27E Advances in GC
  - 27F Gas-Solid Chromatography
  - Questions and Problems
- Chapter 28: High-Performance Liquid Chromatography
  - 28A Scope of HPLC
  - 28B Column Efficiency in LC
  - 28C Instrumentation
  - 28D Partition Chromatography
  - 28E Adsorption Chromatography
  - 28F Ion Chromatography
  - 28G Size-Exclusion Chromatography
  - 28H Affinity Chromatography
  - 28I Thin-Layer Chromatography
  - Questions and Problems
- Chapter 29: Supercritical Fluid Chromatography and Extraction
  - 29A Properties of Supercritical Fluids
  - 29B Supercritical Fluid Chromatography
  - 29C Supercritical Fluid Extraction
  - Questions and Problems
- Chapter 30: Capillary Electrophoresis, Electrochromatography, and Field-Flow Fractionation
  - 30A An Overview of Electrophoresis
  - 30B Capillary Electrophoresis
  - 30C Applications of CE
  - 30D Packed Column Electrochromatography
  - 30E Field-Flow Fractionation
  - Questions and Problems
  - Instrumental Analysis in Action - The Bisphenol A Controversy
Section 6: Miscellaneous Methods
- Chapter 31: Thermal Methods
  - 31A Thermogravimetric Analysis
  - 31B Differential Thermal Analysis
  - 31C Differential Scanning Calorimetry
  - 31D Microthermal Analysis
  - Questions and Problems
- Chapter 32: Radiochemical Methods
  - 32A Radioactive Nuclides
  - 32B Instrumentation
  - 32C Neutron Activation Methods
  - 32D Isotope Dilution Methods
  - Questions and Problems
- Chapter 33: Automated Methods of Analysis
  - 33A Overview
  - 33B Flow Injection Analysis
  - 33C Microfluidics
  - 33D Discrete Automatic Systems
  - Questions and Problems
- Chapter 34: Particle Size Determination
  - 34A Introduction to Particle Size Analysis
  - 34B Low-Angle Laser Light Scattering
  - 34C Dynamic Light Scattering
  - 34D Photosedimentation
  - Questions and Problems
  - Instrumental Analysis in Action - The John F. Kennedy Assassinaton
Appendix 1: Evaluation of Analytical Data
Appendix 2: Activity Coefficients
Appendix 3: Some Standard and Formal Electrode Potentials
Appendix 4: Compounds Recommended for the Preparation of Standard Solutions of Some Common Elements
Answers to Selected Problems
Index

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Gerð : 208
Höfundur : 6270
Útgáfuár : 2017
Leyfi : 380

5.390 kr.

Principles of Instrumental Analysis

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Principles of Instrumental Analysis

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UM RAFBÆKUR Á HEIMKAUP.IS

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