Efnisyfirlit

• Cover
• Preface to the Eleventh Edition
• Text Figures: Quick Reference Guide
• Chapter 1: Safety First, Last, and Always
  • Accidents Will Not Happen
  • Disposing of Waste
  • Safety Data Sheets
  • Green Chemistry
  • An iBag for Your iThing
  • Exercises
• Chapter 2: Keeping a Notebook
  • A Technique Experiment
  • A Synthesis Experiment
  • The Six Maybe Seven Elements in Your Experimental Write-up
  • The Acid Test
  • Notebook Mortal Sin
  • Calculation of Percent Yield (Not Yeild!)
  • Estimation Is Your Friend
  • Notes From My Bench
  • Exercises
• Chapter 3: Mining Your Own Data
  • Google and the Wiki
  • The Terphenyl Anomaly
  • Exercises
• Chapter 4: Jointware
  • Stoppers with Only One Number
  • Another Episode of Love of Laboratory
  • Hall of Blunders and Things Not Quite Right
  • The O-Ring and Cap Branch Out
  • Greasing the Joints
  • Storing Stuff and Sticking Stoppers
  • Corking a Vessel
• Chapter 5: Microscale Jointware
  • Microscale: A Few Words
  • Uh-Oh Rings
  • The O-Ring Cap Seal
  • The Comical Vial (That’s Conical!)
  • The Microscale Drying Tube
  • Gas Collection Apparatus
• Chapter 6: Other Interesting Equipment
  • Funnels, and Beakers, and Flasks—Oh My!
  • The Flexible Double-Ended Stainless Steel Spatula
• Chapter 7: Pipet Tips
  • Pre-Preparing Pasteur Pipets
  • Pipet Cutting
  • Pipet Filtering—Liquids
  • Pipet Filtering—Solids
• Chapter 8: Syringes, Needles, and Septa
  • The Rubber Septum
• Chapter 9: Clean and Dry
  • Drying Your Glassware When You Don’t Need To
  • Drying Your Glassware When You Do Need To
• Chapter 10: Drying Agents
  • Typical Drying Agents
  • Using a Drying Agent
  • Following Directions and Losing Product Anyway
  • Drying Agents: Microscale
  • Drying in Stages: The Capacity and Efficiency of Drying Agents
  • Exercises
• Chapter 11: On Products
  • Solid Product Problems
  • Liquid Product Problems
  • The Sample Vial
  • Hold It! Don’t Touch That Vial
• Chapter 12: The Melting-Point Experiment
  • Sample Preparation
  • Melting-Point Hints
  • The Mel-Temp Apparatus
  • The SRS DigiMelt
  • The Fisher-Johns Apparatus
  • The Thomas-Hoover Apparatus
  • Using the Thiele Tube
  • Exercises
• Chapter 13: Recrystallization
  • Finding a Good Solvent
  • General Guidelines for a Recrystallization
  • Gravity Filtration
  • The Buchner Funnel and Filter Flask
  • The Hirsch Funnel and Friends
  • Activated Charcoal
  • The Water Aspirator: A Vacuum Source
  • The Water Trap
  • Working with a Mixed-Solvent System—The Good Part
  • A Mixed-Solvent System—The Bad Part
  • Salting Out
  • World-Famous Fan-Folded Fluted Paper
  • Exercises
• Chapter 14: Recrystallization: Microscale
  • Isolating the Crystals
  • Craig Tube Filtration
  • Centrifuging the Craig Tube
• Chapter 15: Extraction and Washing
  • Never-Ever Land
  • Starting an Extraction
  • Dutch Uncle Advice
  • The Separatory Funnel
  • How to Extract and Wash What
  • Exercises
• Chapter 16: Extraction and Washing: Microscale
  • Mixing
  • Separation: Removing the Bottom Layer (Fig. 16.1)
  • Separation: Removing the Top Layer (Fig. 16.2)
  • Separation: Removing Both Layers
• Chapter 17: Sources of Heat
  • Boiling Stones
  • The Steam Bath
  • The Bunsen Burner
  • The Heating Mantle
  • Proportional Heaters and Stepless Controllers
  • Exercise
• Chapter 18: Clamps and Clamping
  • Clamping a Distillation Setup
  • Clipping a Distillation Setup
• Chapter 19: Distillation
  • Distillation Notes
  • Class 1: Simple Distillation (Fig. 19.1)
  • The Distillation Example
  • The Distillation Mistake
  • Class 2: Vacuum Distillation
  • Class 3: Fractional Distillation
  • Azeotropes
  • Class 4: Steam Distillation
  • Steam Distillation Notes
  • Simulated Bulb-to-Bulb Distillation: Fakelrohr
  • Exercises
• Chapter 20: Microscale Distillation
  • Like the Big Guy
  • Microscale Distillation II: The Hickman Still
• Chapter 21: The Rotary Evaporator
  • Exercises
• Chapter 22: Reflux and Addition
  • Standard Reflux
  • A Dry Reflux
  • Addition and Reflux
  • Exercise
• Chapter 23: Reflux: Microscale
  • Addition and Reflux: Microscale
• Chapter 24: Sublimation
• Chapter 25: Microscale Boiling Point
  • Microscale Boiling Point
  • Ultramicroscale Boiling Point
• Chapter 26: Chromatography
  • Adsorbents
  • Separation or Development
  • The Eluatropic Series
• Chapter 27: Thin-Layer Chromatography: TLC
  • We Don’t Make Our Own TLC Plates Any More, But…
  • The Plate Spotter
  • Spotting the Plates
  • Developing a Plate
  • Visualization
  • Interpretation
  • Multiple Spotting
  • Cospotting
  • Other TLC Problems
  • Preparative TLC
  • Exercises
• Chapter 28: Wet-Column Chromatography
  • Preparing the Column
  • Compounds on the Column
  • Visualization and Collection
  • Wet-Column Chromatography: Microscale
  • Flash Chromatography
  • Microscale Flash Chromatography
  • Exercises
• Chapter 29: Refractometry
  • The Abbé Refractometer
  • Before Using the Abbé Refractometer: A Little Practice
  • Using the Abbé Refractometer
  • Refractometry Hints
• Chapter 30: Gas Chromatography
  • The Mobile Phase: Gas
  • GC Sample Preparation
  • GC Sample Introduction
  • Sample in the Column
  • Sample at the Detector
  • Electronic Interlude
  • Sample on the Computer
  • Parameters, Parameters
  • Exercises
• Chapter 31: HP Liquid Chromatography
  • The Mobile Phase: Liquid
  • HPLC Sample Preparation
  • HPLC Sample Introduction
  • Sample in the Column
  • Sample at the Detector
  • Sample on the Computer
  • Parameters, Parameters
  • Exercises
• Chapter 32: Infrared Spectroscopy: (And a Bit Of UV-VIS, Too)
  • Molecules as Balls on Springs
  • AH, Quantum Mechanics
  • The Dissonant Oscillator
  • But Wait! There’s More
  • More Complicated Molecules
  • Correlation Tables to the Rescue
  • Troughs and Reciprocal Centimeters
  • Some Functional Group Analysis
  • A Systematic Interpretation
  • IR Sample Preparation
  • Running the Spectrum
  • Interpreting IR Spectra—Finishing Touches
  • The Fourier Transform Infrared (FTIR)
  • A Reflectance Attachment: Something to Think About
  • And UV-VIS Too!
  • Electrons Get to Jump
  • Instrument Configuration
  • Exercises
• Chapter 33: Nuclear Magnetic Resonance
  • Nuclei Have Spin, Too
  • The Magnetic Catch
  • Everybody Line Up, Flip, and Relax
  • A More Sensitive Census
  • The Chemical Shift
  • T for One and Two
  • Be It Better Resolved…
  • Incredibly Basic FT-NMR
  • NMR Sample Preparation
  • Some NMR Terms and Interpretations
  • Exercises
• Index
• End User License Agreement

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